
New TopShim run:

version = topshim 4.4.0
date = 2026-09-28
time = 14:07:30.082
command = topshim 1d optsolvent coil=1H optsolvent tuneaoff hrmas

HRMAS SHIMMING

Parameters:

probe = Z180004_0001
angle PHI = 270.5 degree
solvent = H2O+D2O
shim nucleus = 1H
nucleus optimised for = 1H
o1p (from lock) = 4.70 ppm

Results:

Iteration 1: FWHM Before=16.5 Hz, Target= 0.5 Hz, After= 9.1 Hz
Iteration 2: FWHM Before= 9.1 Hz, Target= 3.8 Hz, After= 0.6 Hz
Iteration 3: FWHM Before= 0.6 Hz, Target= 0.3 Hz, After=202.2 Hz
Iteration 4: FWHM Before=202.2 Hz, Target= 3.3 Hz, After=33.0 Hz
Iteration 5: FWHM Before=33.0 Hz, Target= 3.1 Hz, After= 2.8 Hz
Using the best result as the final shim state.

Lineshape quality factor (1D spectrum, MAS) = 11.4


Unusually slow convergence behaviour detected during shimming.
This may be indicative of an incorrect mounting angle being used!
1. Please perform 'topshim calreset'
2. Restart topshim
3. Enter the correct value for the mounting angle


MAS shims:
Z'	-11290
Z2'	+53298
Z3'	+52382
Z4'	+0


duration = 1 min 55 sec
completed successfully
finished Mon Sep 28 14:09:24 2026


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