
New TopShim run:

version = topshim 4.4.0
date = 2026-09-29
time = 16:43:47.671
command = topshim 1d optsolvent coil=1H optsolvent tunea hrmas

HRMAS SHIMMING

Parameters:

probe = Z180004_0001
angle PHI = 270.5 degree
solvent = H2O+D2O
shim nucleus = 1H
nucleus optimised for = 1H
o1p (from lock) = 4.70 ppm

Results:

Iteration 1: FWHM Before= 0.2 Hz, Target= 0.2 Hz, After= 0.5 Hz
Iteration 2: FWHM Before= 0.5 Hz, Target= 0.2 Hz, After= 0.3 Hz
Iteration 3: FWHM Before= 0.3 Hz, Target= 0.2 Hz, After= 0.4 Hz
Iteration 4: FWHM Before= 0.4 Hz, Target= 0.2 Hz, After= 0.3 Hz
Iteration 5: FWHM Before= 0.3 Hz, Target= 0.2 Hz, After= 0.4 Hz
Rejecting all results and reverting to the initial shim state.

Lineshape quality factor (1D spectrum, MAS) = 1.75


Unusually slow convergence behaviour detected during shimming.
This may be indicative of an incorrect mounting angle being used!
1. Please perform 'topshim calreset'
2. Restart topshim
3. Enter the correct value for the mounting angle


MAS shims:
Z'	-15913
Z2'	+92454
Z3'	-46373
Z4'	+0


duration = 1 min 42 sec
completed successfully
finished Tue Sep 29 16:45:29 2026


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