Mestrelab Research S.L. o j eBMS Shell Dlg 2@22{pageIndex}?$MS Shell Dlg 2@22{name, 0}? { yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709bDocument Items ParentshipC|(Dƙ:. saisankarguptakb%myF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709bDocument Items ParentshipC|(Dƙ:. saisankarguptakb%yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709bDocument Items ParentshipC|(Dƙ:. saisankarguptakb%yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709bDocument Items ParentshipC|(Dƙ:. saisankarguptakb%njyF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709bDocument Items ParentshipC|(Dƙ:. saisankarguptakb%yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709bDocument Items ParentshipC|(Dƙ:. saisankarguptakb% yF4,&!vuw.leidenuniv.nl& MestReNovaWindows 10 Version 2009W0045709. Save DocumentC|(Dƙ:. saisankarguptakb%" MestReNova Mnova Name MestReNova$ 15.0.0-34764! Mnova Version 15.0.0-34764o W//vuw/Personal$/Homes/s/saisankarguptakb/Downloads/DOSY_gamma_Cyclodextrin_500_01.mnovah File NameW//vuw/Personal$/Homes/s/saisankarguptakb/Downloads/DOSY_gamma_Cyclodextrin_500_01.mnova. QUuidC|(Dƙ:.0ID&{fa43a87c-281a-44c6-993a-2ef39ebc12fb}yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709bDocument Items ParentshipC|(Dƙ:. saisankarguptakb%/hyF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709bDocument Items ParentshipC|(Dƙ:. saisankarguptakb%2yF4,&!vuw.leidenuniv.nl& MestReNovaWindows 10 Version 2009W0045709. Save DocumentC|(Dƙ:. saisankarguptakb%3<" MestReNova Mnova Name MestReNova$ 15.0.0-34764! Mnova Version 15.0.0-34764o W//vuw/Personal$/Homes/s/saisankarguptakb/Downloads/DOSY_gamma_Cyclodextrin_500_01.mnovah File NameW//vuw/Personal$/Homes/s/saisankarguptakb/Downloads/DOSY_gamma_Cyclodextrin_500_01.mnova. QUuidC|(Dƙ:.0ID&{fa43a87c-281a-44c6-993a-2ef39ebc12fb}nMestReNova15.0.0-34764C|(Dƙ:.HyF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709Create Item (Text)HI\OƌK[F saisankarguptakb% Type NMR DOSYSubtype PeaksName TextID &{48fb4992-185c-4fc6-8c4b-cc5babc2da46} ItemyF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709MEdit text itemHI\OƌK[F saisankarguptakb%r r

#

Label

Position (ppm)

Intensity

Fit 1

1

1

P(5.04 ppm)

5.041

3.61e+05

A=366738 (1082.58)
D=2.00794e-06 cm2/s (1.31167e-08)

2

2

P(5.03 ppm)

5.034

348608.502

A=346481 (1007.76)
D=2.04498e-06 cm2/s (1.31403e-08)

3

3

P(4.7 ppm)

4.701

2.436e+06

A=2.57075e+06 (23697.1)
D=1.63267e-05 cm2/s (2.92165e-07)

4

4

P(3.88 ppm)

3.881

158809.853

A=162324 (899.694)
D=2.02361e-06 cm2/s (2.48023e-08)

5

5

P(3.86 ppm)

3.862

333419.271

A=336149 (580.406)
D=2.05495e-06 cm2/s (7.83518e-09)

6

6

P(3.84 ppm)

3.843

211863.498

A=212577 (762.354)
D=2.07418e-06 cm2/s (1.64127e-08)

7

7

P(3.82 ppm)

3.822

62457.005

A=63196.4 (539.393)
D=1.94255e-06 cm2/s (3.68105e-08)

8

8

P(3.8 ppm)

3.798

7.78e+05

A=781877 (1683.84)
D=2.02518e-06 cm2/s (9.64385e-09)

9

9

P(3.78 ppm)

3.78

2.34e+05

A=234206 (926.569)
D=2.02563e-06 cm2/s (1.77196e-08)

10

10

P(3.59 ppm)

3.595

241343.294

A=241139 (1046.62)
D=1.99841e-06 cm2/s (1.92031e-08)

11

11

P(3.59 ppm)

3.587

221941.222

A=220684 (907.632)
D=1.9803e-06 cm2/s (1.80476e-08)

12

12

P(3.57 ppm)

3.575

208610.429

A=207480 (819.293)
D=1.97832e-06 cm2/s (1.73121e-08)

13

13

P(3.57 ppm)

3.567

195093.342

A=195322 (651.367)
D=2.00275e-06 cm2/s (1.47835e-08)

14

14

P(3.54 ppm)

3.536

126756.965

A=128207 (309.353)
D=1.99577e-06 cm2/s (1.06629e-08)

15

15

P(3.52 ppm)

3.518

209279.535

A=210049 (450.354)
D=2.02388e-06 cm2/s (9.59548e-09)

16

16

P(3.5 ppm)

3.499

97555.895

A=97070.1 (322.895)
D=2.0389e-06 cm2/s (1.49874e-08)

rTextr

#

Label

Position (ppm)

Intensity

Fit 1

1

1

P(5.04 ppm)

5.041

3.61e+05

A=366738 (?1082.58)
D=2.00794e-06 cm2/s (?1.31167e-08)

2

2

P(5.03 ppm)

5.034

348608.502

A=346481 (?1007.76)
D=2.04498e-06 cm2/s (?1.31403e-08)

3

3

P(4.7 ppm)

4.701

2.436e+06

A=2.57075e+06 (?23697.1)
D=1.63267e-05 cm2/s (?2.92165e-07)

4

4

P(3.88 ppm)

3.881

158809.853

A=162324 (?899.694)
D=2.02361e-06 cm2/s (?2.48023e-08)

5

5

P(3.86 ppm)

3.862

333419.271

A=336149 (?580.406)
D=2.05495e-06 cm2/s (?7.83518e-09)

6

6

P(3.84 ppm)

3.843

211863.498

A=212577 (?762.354)
D=2.07418e-06 cm2/s (?1.64127e-08)

7

7

P(3.82 ppm)

3.822

62457.005

A=63196.4 (?539.393)
D=1.94255e-06 cm2/s (?3.68105e-08)

8

8

P(3.8 ppm)

3.798

7.78e+05

A=781877 (?1683.84)
D=2.02518e-06 cm2/s (?9.64385e-09)

9

9

P(3.78 ppm)

3.78

2.34e+05

A=234206 (?926.569)
D=2.02563e-06 cm2/s (?1.77196e-08)

10

10

P(3.59 ppm)

3.595

241343.294

A=241139 (?1046.62)
D=1.99841e-06 cm2/s (?1.92031e-08)

11

11

P(3.59 ppm)

3.587

221941.222

A=220684 (?907.632)
D=1.9803e-06 cm2/s (?1.80476e-08)

12

12

P(3.57 ppm)

3.575

208610.429

A=207480 (?819.293)
D=1.97832e-06 cm2/s (?1.73121e-08)

13

13

P(3.57 ppm)

3.567

195093.342

A=195322 (?651.367)
D=2.00275e-06 cm2/s (?1.47835e-08)

14

14

P(3.54 ppm)

3.536

126756.965

A=128207 (?309.353)
D=1.99577e-06 cm2/s (?1.06629e-08)

15

15

P(3.52 ppm)

3.518

209279.535

A=210049 (?450.354)
D=2.02388e-06 cm2/s (?9.59548e-09)

16

16

P(3.5 ppm)

3.499

97555.895

A=97070.1 (?322.895)
D=2.0389e-06 cm2/s (?1.49874e-08)

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Data

"Text

Data

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Data

yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709Cut Item (Text)س BFA] saisankarguptakb% f Name TextID &{bcd8b30b-0442-46c0-94c1-eda7415d8d92} ItemyF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709rImport Item (NMR Spectrum)7RKlh.> saisankarguptakb% Type 2D Title 0DOSY Transform 1H_DOSY_gamma-cyclodextrin.19.serSubtype 1HUnknown, DOSY-UnknownName NMR SpectrumID &{37521eae-e08b-4bb9-95a7-e66c689f2e3e} ItemyF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709 Set Property7RKlh.> saisankarguptakb%1 traces.horizontal.visible)Propertytraces.horizontal.visible Valuetrue  anonymous(a2DSpc,aHTraceArr,aVTraceArr)@nmrAutoAttachTraces.qs:74 nnmrAutoAttachTraces(aItemId)@nmrAutoAttachTraces.qs:119Script BacktraceyF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709 Traces Setup7RKlh.> saisankarguptakb%. QUuidAvO>N Attach Horizontal External Trace&{af881f9a-c9c6-4176-afec-eec2fc4f3eca}  anonymous(a2DSpc,aHTraceArr,aVTraceArr)@nmrAutoAttachTraces.qs:75 nnmrAutoAttachTraces(aItemId)@nmrAutoAttachTraces.qs:119Script BacktraceyF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709 Show Traces7RKlh.> saisankarguptakb%  Horizontaltrue VerticaltrueyF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709Increase Intensity7RKlh.> saisankarguptakb% PٍY Threshold 29199353856yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709Set Trace Intensity7RKlh.> saisankarguptakb% VerticalTraceVertical ?Ratio1 IncreasetrueyF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709 Cut range7RKlh.> saisankarguptakb%B( [9.6557,11.2483]X Range[9.6557,11.2483]+ [1.06707e-08,1e-05]"Y Range[1.06707e-08,1e-05]yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709 Cut range7RKlh.> saisankarguptakb%) [7.52212,11.2483] X Range[7.52212,11.2483]+ [1e-12,2.47584e-11]"Y Range[1e-12,2.47584e-11]yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709 Cut range7RKlh.> saisankarguptakb%z* [-1.24818,1.22098]!X Range[-1.24818,1.22098]1 [3.63387e-09,1.05996e-08](Y Range[3.63387e-09,1.05996e-08]yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709Set Trace Intensity7RKlh.> saisankarguptakb% VerticalTraceVertical ?Ratio1 IncreasetrueyF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709tSet NMR Spectrum Properties7RKlh.> saisankarguptakb%={ TitleVisible2D Legend Width@I TitleVisible2D Legend Width@Hׯ` PropertiesyF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709rDelete Item (NMR Spectrum)7RKlh.> saisankarguptakb% x Type 2D Title 0DOSY Transform 1H_DOSY_gamma-cyclodextrin.19.serSubtype 1HUnknown, DOSY-UnknownName NMR SpectrumID &{37521eae-e08b-4bb9-95a7-e66c689f2e3e} ItemyF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709 Create PageůbHH- saisankarguptakb%r  At2yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709T Delete PageůbHH- saisankarguptakb% xyF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709Create Item (Text)ڗ \Bo$ĝ saisankarguptakb% . Type DOSYSubtype ParametersName TextID &{da970de2-5cc6-426f-aff0-c024c49db41e} ItemyF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709Move selectionڗ \Bo$ĝ saisankarguptakb%  Text Item TypeText @ x6116 @ y5838yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709DEdit text itemڗ \Bo$ĝ saisankarguptakb% "G "/

Name

Value

Data

? (s)

0.1799

? (1/Gs)

26751.918082378525

d (s)

0.0024

?

1

Parameters

Auto Scale

true

Data Scaling

No Scaling

Experiment Type

Diffusion

Ignore First Point

false

Max Diffusion

0.0001

Min Diffusion

1e-06

Number of Diffusion Points

128

Peak Options

Auto Correct Positions

true

Confidence Interval

95 %

Fit Mode

Normal

Numer of Exponentials

1

Units

m^2/sec

";Text"/

Name

Value

Data

? (s)

0.1799

? (1/G?s)

26751.918082378525

d (s)

0.0024

?

1

Parameters

Auto Scale

true

Data Scaling

No Scaling

Experiment Type

Diffusion

Ignore First Point

false

Max Diffusion

0.0001

Min Diffusion

1e-06

Number of Diffusion Points

128

Peak Options

Auto Correct Positions

true

Confidence Interval

95 %

Fit Mode

Normal

Numer of Exponentials

1

Units

m^2/sec

yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709DEdit text itemڗ \Bo$ĝ saisankarguptakb% "G "/

Name

Value

Data

? (s)

0.1799

? (1/Gs)

26751.918082378525

d (s)

0.0024

?

1

Parameters

Auto Scale

true

Data Scaling

No Scaling

Experiment Type

Diffusion

Ignore First Point

false

Max Diffusion

0.0001

Min Diffusion

1e-06

Number of Diffusion Points

128

Peak Options

Auto Correct Positions

true

Confidence Interval

95 %

Fit Mode

Normal

Numer of Exponentials

1

Units

m^2/sec

";Text"/

Name

Value

Data

? (s)

0.1799

? (1/G?s)

26751.918082378525

d (s)

0.0024

?

1

Parameters

Auto Scale

true

Data Scaling

No Scaling

Experiment Type

Diffusion

Ignore First Point

false

Max Diffusion

0.0001

Min Diffusion

1e-06

Number of Diffusion Points

128

Peak Options

Auto Correct Positions

true

Confidence Interval

95 %

Fit Mode

Normal

Numer of Exponentials

1

Units

m^2/sec

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Name

Value

Data

? (s)

0.1799

? (1/Gs)

26751.918082378525

d (s)

0.0024

?

1

Parameters

Auto Scale

true

Data Scaling

No Scaling

Experiment Type

Diffusion

Ignore First Point

false

Max Diffusion

0.0001

Min Diffusion

1e-06

Number of Diffusion Points

128

Peak Options

Auto Correct Positions

true

Confidence Interval

95 %

Fit Mode

Normal

Numer of Exponentials

1

Units

m^2/sec

";Text"/

Name

Value

Data

? (s)

0.1799

? (1/G?s)

26751.918082378525

d (s)

0.0024

?

1

Parameters

Auto Scale

true

Data Scaling

No Scaling

Experiment Type

Diffusion

Ignore First Point

false

Max Diffusion

0.0001

Min Diffusion

1e-06

Number of Diffusion Points

128

Peak Options

Auto Correct Positions

true

Confidence Interval

95 %

Fit Mode

Normal

Numer of Exponentials

1

Units

m^2/sec

yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709DEdit text itemъgLJYE^i saisankarguptakb% "G "/

Name

Value

Data

? (s)

0.1799

? (1/Gs)

26751.918082378525

d (s)

0.0024

?

1

Parameters

Auto Scale

true

Data Scaling

No Scaling

Experiment Type

Diffusion

Ignore First Point

false

Max Diffusion

0.0001

Min Diffusion

1e-06

Number of Diffusion Points

128

Peak Options

Auto Correct Positions

true

Confidence Interval

95 %

Fit Mode

Normal

Numer of Exponentials

1

Units

m^2/sec

";Text"/

Name

Value

Data

? (s)

0.1799

? (1/G?s)

26751.918082378525

d (s)

0.0024

?

1

Parameters

Auto Scale

true

Data Scaling

No Scaling

Experiment Type

Diffusion

Ignore First Point

false

Max Diffusion

0.0001

Min Diffusion

1e-06

Number of Diffusion Points

128

Peak Options

Auto Correct Positions

true

Confidence Interval

95 %

Fit Mode

Normal

Numer of Exponentials

1

Units

m^2/sec

yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709Move selectionъgLJYE^i saisankarguptakb% 4 Text Item TypeText @+ x4651 @X y5976yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709Move selectionъgLJYE^i saisankarguptakb% y[ Text Item TypeText @ x4747 @v y7798yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709Paste Item (Text)ъgLJYE^i saisankarguptakb%  Type DOSYSubtype ParametersName TextID &{d18a674c-bbde-4a59-a108-1ae1455e699b} ItemyF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709Move selectionъgLJYE^i saisankarguptakb%  Text Item TypeText @& x6438 @ y6162yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709Cut Item (Text)ъgLJYE^i saisankarguptakb%04 Type DOSYSubtype ParametersName TextID &{d18a674c-bbde-4a59-a108-1ae1455e699b} ItemyF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709Create Item (Text))u?BB saisankarguptakb% . Type DOSYSubtype ParametersName TextID &{da970de2-5cc6-426f-aff0-c024c49db41e} ItemyF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709Move selection)u?BB saisankarguptakb%  Text Item TypeText @ x6116 @ y5838yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709DEdit text item)u?BB saisankarguptakb% "G "/

Name

Value

Data

? (s)

0.1799

? (1/Gs)

26751.918082378525

d (s)

0.0024

?

1

Parameters

Auto Scale

true

Data Scaling

No Scaling

Experiment Type

Diffusion

Ignore First Point

false

Max Diffusion

0.0001

Min Diffusion

1e-06

Number of Diffusion Points

128

Peak Options

Auto Correct Positions

true

Confidence Interval

95 %

Fit Mode

Normal

Numer of Exponentials

1

Units

m^2/sec

";Text"/

Name

Value

Data

? (s)

0.1799

? (1/G?s)

26751.918082378525

d (s)

0.0024

?

1

Parameters

Auto Scale

true

Data Scaling

No Scaling

Experiment Type

Diffusion

Ignore First Point

false

Max Diffusion

0.0001

Min Diffusion

1e-06

Number of Diffusion Points

128

Peak Options

Auto Correct Positions

true

Confidence Interval

95 %

Fit Mode

Normal

Numer of Exponentials

1

Units

m^2/sec

yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709DEdit text item)u?BB saisankarguptakb% "G "/

Name

Value

Data

? (s)

0.1799

? (1/Gs)

26751.918082378525

d (s)

0.0024

?

1

Parameters

Auto Scale

true

Data Scaling

No Scaling

Experiment Type

Diffusion

Ignore First Point

false

Max Diffusion

0.0001

Min Diffusion

1e-06

Number of Diffusion Points

128

Peak Options

Auto Correct Positions

true

Confidence Interval

95 %

Fit Mode

Normal

Numer of Exponentials

1

Units

m^2/sec

";Text"/

Name

Value

Data

? (s)

0.1799

? (1/G?s)

26751.918082378525

d (s)

0.0024

?

1

Parameters

Auto Scale

true

Data Scaling

No Scaling

Experiment Type

Diffusion

Ignore First Point

false

Max Diffusion

0.0001

Min Diffusion

1e-06

Number of Diffusion Points

128

Peak Options

Auto Correct Positions

true

Confidence Interval

95 %

Fit Mode

Normal

Numer of Exponentials

1

Units

m^2/sec

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26751.918082378525

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#

Spectrum

G (G/cm)

B (s/cm^2)

1

1

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

2.408

4280.957

2

2

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

3.805

10689.004

3

3

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

5.203

19986.446

4

4

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

6.601

32169.728

5

5

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

7.999

47238.85

6

6

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

9.397

65193.812

7

7

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

10.795

86034.614

8

8

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

12.193

109761.256

9

9

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

13.591

136373.738

10

10

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

14.989

165872.061

11

11

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

16.387

198256.223

12

12

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

17.784

233499.965

13

13

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

19.182

271653.744

14

14

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

20.58

312693.362

15

15

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

21.978

356618.82

16

16

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

23.376

403430.119

17

17

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

24.774

453127.257

18

18

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

26.172

505710.236

19

19

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

27.57

561179.055

20

20

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

28.968

619533.714

21

21

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

30.366

680774.212

22

22

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

31.763

744853.65

23

23

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

33.161

811863.765

24

24

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

34.559

881759.72

25

25

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

35.957

954541.514

26

26

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

37.355

1.03e+06

27

27

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

38.753

1.109e+06

28

28

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

40.151

1.19e+06

29

29

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

41.549

1.275e+06

30

30

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

42.947

1361738.09

31

31

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

44.345

1.452e+06

32

32

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

45.743

1.545e+06

Text

#

Spectrum

G (G/cm)

B (s/cm^2)

1

1

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

2.408

4280.957

2

2

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

3.805

10689.004

3

3

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

5.203

19986.446

4

4

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

6.601

32169.728

5

5

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

7.999

47238.85

6

6

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

9.397

65193.812

7

7

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

10.795

86034.614

8

8

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

12.193

109761.256

9

9

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

13.591

136373.738

10

10

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

14.989

165872.061

11

11

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

16.387

198256.223

12

12

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

17.784

233499.965

13

13

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

19.182

271653.744

14

14

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

20.58

312693.362

15

15

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

21.978

356618.82

16

16

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

23.376

403430.119

17

17

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

24.774

453127.257

18

18

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

26.172

505710.236

19

19

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

27.57

561179.055

20

20

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

28.968

619533.714

21

21

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

30.366

680774.212

22

22

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

31.763

744853.65

23

23

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

33.161

811863.765

24

24

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

34.559

881759.72

25

25

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

35.957

954541.514

26

26

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

37.355

1.03e+06

27

27

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

38.753

1.109e+06

28

28

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

40.151

1.19e+06

29

29

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

41.549

1.275e+06

30

30

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

42.947

1361738.09

31

31

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

44.345

1.452e+06

32

32

1H_DOSY_gamma-cyclodextrin.19.ser 1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 mins

45.743

1.545e+06

yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709Create Item (Text)wlH^KA-̇} saisankarguptakb%2 Type DOSYSubtype ParametersName TextID &{8b9f776c-d016-485e-834b-412dcc87f87d} ItemyF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709Move selectionwlH^KA-̇} saisankarguptakb%2 Text Item TypeText @ x7338 @ y5830yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709Move selectionwlH^KA-̇} saisankarguptakb%2" Text Item TypeText @ x8458 @ y7190yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709DEdit text itemwlH^KA-̇} saisankarguptakb%2"G "/

Name

Value

Data

? (s)

0.1799

? (1/Gs)

26751.918082378525

d (s)

0.0024

?

1

Parameters

Auto Scale

true

Data Scaling

No Scaling

Experiment Type

Diffusion

Ignore First Point

false

Max Diffusion

0.0001

Min Diffusion

1e-06

Number of Diffusion Points

128

Peak Options

Auto Correct Positions

true

Confidence Interval

95 %

Fit Mode

Normal

Numer of Exponentials

1

Units

m^2/sec

";Text"/

Name

Value

Data

? (s)

0.1799

? (1/G?s)

26751.918082378525

d (s)

0.0024

?

1

Parameters

Auto Scale

true

Data Scaling

No Scaling

Experiment Type

Diffusion

Ignore First Point

false

Max Diffusion

0.0001

Min Diffusion

1e-06

Number of Diffusion Points

128

Peak Options

Auto Correct Positions

true

Confidence Interval

95 %

Fit Mode

Normal

Numer of Exponentials

1

Units

m^2/sec

yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709Move selectionwlH^KA-̇} saisankarguptakb%2 Text Item TypeText @ x7835 @ y6680yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709Delete Item (Text)wlH^KA-̇} saisankarguptakb%2 Type DOSYSubtype ParametersName TextID &{8b9f776c-d016-485e-834b-412dcc87f87d} Item* (#=% Y3(66@'>|@r66 (#:(I{@`K~2Y3Y3Y3wm[ (@o0JKume]UAyF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709 Import Item (NMR Spectrum)AvO> saisankarguptakb%mN Type 1D Title !1H_DOSY_gamma-cyclodextrin.19.serSubtype stacked, 1HName NMR SpectrumID &{af881f9a-c9c6-4176-afec-eec2fc4f3eca} Item ^  md5sum19/ vtc_pid_settings 7641af9842fc71de98dd94973e6a0c39uxnmr.par ad9396df5bec60f30fbed74bc52b1590uxnmr.info eab26a435c1a00856024b7683d69edbaspecpar c7a6adc15c0bbe2695e2c8332eed579cshimvalues 84db545fbac9ab4c0ed7a25d6ea6ab48ser ac57349a6d6cf7ab3853ce75365dd067 scon2 18270a14ce2659d32140a1e70f067c8f(pulseprogram.precomp bb68db30e0e1a516fa191ad30d9e9287 pdata/1/ title d2d85eae790aed05aea52c68f7c2af88thumb.png 1cffee7e870356db713fab767bd63800t1t2.dx c0dae01c800bd992d7b31e279a1e981bt1peaks.txt 4ae9abcd3284aa610fd1df5382c0ef3bt1peaks 2402f92a11c1b3c0fab447a2a5646c2b t1par 45145dcdf7e0ec91bab44645b9a6340ct1ints.txt 591ad21d810a104e519e72f1e308ef00 t1ints 399875d9d398692ac89c5409c9a1fd07t1elim.txt fba280d3844f77d56a60d5f4e6079df4 t1elim 348a9791dc41b89796ec3808b5b5262ft1_disp 04a9f5a5a82ec69d2af0c65146622cfdpt1t2.par 57d7e7187f83de8954ffcca5993f4489 procs f76c44cb2f34cbc8c9c39d0621b58f81 proc2s 99050c9a95e789e4d4576f3d32bec2f7 proc2 95da16c453cba0d835362d261d5d93dbproc a631102aedd5829e1b4f5e1db614c170ppmt1t2.txt 6f94943349b96c7e29812e35ff09a10foutd d4931e87f2eea6c883e133ab9dd43864 intrng 7a1139044c11df1b931eaf666dc4b7b4dt1t2.txt bbee9b905b29c0ca5e220c96486ce2cfdosy 2f2628d4bc81b5c2bf5dff8ad0a89270ct1t2.txt ddb9c27957fd413de7f95c39bb49ac66clevels 4fe518741a624963994166845948eb83baslpnts 76dd2c9326cdb1a0db64e2694d3ef218auditp.txt 1e1db26044027014eff99093155baf26format.temp 2bc51ccb148a4d6dc8726887684bea39format.ased 415c61eed201f85239a0ff11dfa4706adifflist 0879f772345917ce39a40a52f5196c43audita.txt ee744ed61a8f6e6c83bd6d86789934b0 adcInfo_TRX1.xml 3bde81503b9ba7b84758c7149776560e acqus 3151d1ae54e547b300a7a66cebd19c78 acqum fba1f39641b533d9090c078ab0607af0 acqu2s f1d20bc2d4e83376e62cb3e8414e7af4 acqu2 47c03e5255e80cba6648ae05663c90b0acqu 624461a41d060294998010a8a2361e80Filename J:/ResearchData/FWN/LIC/NMR_DATA/all_nmr_data/av500/data/nmrafd/nmr/1H_DOSY_gamma-cyclodextrin/19/serMetadatayF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709D ProcessingAvO> saisankarguptakb%o  PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 1 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 2 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 3 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 4 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 5 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 6 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 7 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 8 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 9 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 10 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 11 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 12 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 13 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 14 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 15 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 16 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 17 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 18 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 19 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 20 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 21 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 22 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 23 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 24 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 25 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 26 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 27 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 28 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 29 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 30 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 31 PCf1PH1NɴPH0Fa Method ImportedLP Optionsf1SizeGroup Delay Method LinearPhaseShiftFT Propertiesf1QuadratureApodizationf1Exponential321? Parameters 32yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709Increase IntensityAvO> saisankarguptakb%+ [-5646.62, 61611.3] Scale[-5646.62, 61611.3]yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709 Cut rangeAvO> saisankarguptakb%T) [6.11728,11.2484] X Range[6.11728,11.2484]yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709 Cut rangeAvO> saisankarguptakb%h* [-1.24818,2.74489]!X Range[-1.24818,2.74489]yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709 Cut rangeAvO> saisankarguptakb%) [5.48821,11.2484] X Range[5.48821,11.2484]yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709 Cut rangeAvO> saisankarguptakb%]( [4.02237,4.4156]X Range[4.02237,4.4156]yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709 Cut rangeAvO> saisankarguptakb%v* [-1.24818,3.24456]!X Range[-1.24818,3.24456]yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709 Cut rangeAvO> saisankarguptakb%̊) [5.19765,11.2484] X Range[5.19765,11.2484]yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709 Cut rangeAvO> saisankarguptakb%֞( [4.80031,4.8999]X Range[4.80031,4.8999]yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709 Cut rangeAvO> saisankarguptakb%) [3.98641,4.59508] X Range[3.98641,4.59508]yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709 Cut rangeAvO> saisankarguptakb%* [-1.24818,3.34261]!X Range[-1.24818,3.34261]yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709Decrease IntensityAvO> saisankarguptakb%L( [-15937, 173892]Scale[-15937, 173892]yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709Increase IntensityAvO> saisankarguptakb%d+ [-363.905, 3970.64] Scale[-363.905, 3970.64]yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709Decrease IntensityAvO> saisankarguptakb%* [-16399.2, 178935]Scale[-16399.2, 178935]yF4,&!vuw.leidenuniv.nl MestReNovaWindows 10 Version 2009W0045709Z( Peak PickingAvO> saisankarguptakb%! "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard #1 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard #2 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard #3 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard #4 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard #5 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard #6 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard #7 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard #8 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard #9 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard#10 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard#11 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard#12 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard#13 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard#14 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard#15 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard#16 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard#17 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard#18 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard#19 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard#20 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard#21 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard#22 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard#23 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard#24 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard#25 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard#26 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard#27 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard#28 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard#29 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard#30 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard#31 Parameters "Method ParametersSensitivity@$"Refinement Params Level RawPeak Type PositiveNoise Threshold@$Max PeaksInterpolateAuto Classify Method Standard#32 Parameters#$ "ZZ) Discontinued:LSpareSpinbox1Spare 9?Spare 8?Spare 73?Spare 72?Spare 71?Spare 70?Spare 7?Spare 69?Spare 68?Spare 67?Spare 66?Spare 65?Spare 64?Spare 63?Spare 62?Spare 61?Spare 60?Spare 6?Spare 59?Spare 58?Spare 57?Spare 56?Spare 55?Spare 54?Spare 53?Spare 52?Spare 51?Spare 50?Spare 5?Spare 49?Spare 48?Spare 47?Spare 46?Spare 45?Spare 44?Spare 43?Spare 42?Spare 41?Spare 40?Spare 4?Spare 39?Spare 38?Spare 37?Spare 36?Spare 35?Spare 34?Spare 33?Spare 32?Spare 31?Spare 30?Spare 3?Spare 29?Spare 28?Spare 27?Spare 26?Spare 25@Spare 24?Spare 23?Spare 22?Spare 21?Spare 20?Spare 2?Spare 19?Spare 18?Spare 17?Spare 16?Spare 15?Spare 14?Spare 13?Spare 12?Spare 11?Spare 10?Spare 1?:2D axis resolution: X-nucleus?,2D axis resolution: 1H?.WP) Warnings parameters>> W0021 Max References/Compound@4B> W0020 Min Compound/SolventWater?zG{F> W0019 Max Compound/PrimarySolvent@YF> W0018 Min Compound/PrimarySolvent?zG{B> W0016, W0017 Min Q on PKs count333333B> W0014, W0015 Min Q on EMs count333333N> W0013 Min worst-multiplet probability?4> W0012 Min Q on NUC count333333B> W0009 Min S/N ratio per nuclide@ID> W0008 Max impurities molar ratio?333333<> W0007 Min digital resolution@ >> W0006 Max field inhomogeneity@6> W0005 Min processing size8> W0004 Min acquisition sizeD> W0003 Assumed 1H T1 (for Min.RD)@Version Number 2.0 Build @SF) Static (auxiliary) functionsD> Spec.Metric: peaks pos.tolerance?,RD) Run-Time DebuggingBPopUp (cyc means 'test cycle ID):4> Debugged 2D peak yCenter4> Debugged 2D peak xCenter>> Debugged 2D EM ppmY (0...all)>> Debugged 2D EM ppmX (0...all)2> Debugged 1D peak center<> Debugged 1D EM ppm (0...all)B> Analysis cycle [0 last, -1 all]8PcBc) Phase & BC correction: Weight(-1) = Cm4Tail start: T0@Tail height: Th?:Noise beak up-side factor: Bu@<Noise beak low-side factor: Bl?Mode.Histogram: maximum sizep8Histogram bins per noise RMS@"Edge-cut fraction?Q$Data points to use@ÈCpBC coefficients(KI) Known ImpuritiesBFlag those that might be present:PFF) Nmr Parameters Estimates and Fitting FlagsB> Minimum ASV quality for fitting?ə<2D) 2D Peaks Picking | Editing0> V/H strip width factor?2> Top/Bottom Hsqc margins?<> T1-noise intensity threshold?333333D> PP sensitivity in ASV (no touch)@(> Misalign tolerance?07) Multiplets@> qNMR: Minimum nuclei threshold?ٙ>> Principal peaks relative area?8> Maximum integral errors 1H?ə:> Maximum integral errors 13C?D> Inter-multiplet weight threshold?@> Inter-multiplet default gap 1H@2 06) PP/RB/SG/GSD<> Resolution correction factor?0> Peak picking threshold@<> GSD peak splitting threshold?6> GSD fitting cycles in ASV*> 1D Peaks shape type05) MoleculePredictions 1H0* Minimum 1H shift error?ə@* Max shift error factor: PEF_1H@B* Max J-HH error factor: PEF_J-HH?8* Extra PEF factor for dia H?<* Default J-HH relative error:?Predictions 13C2* Minimum 13C shift error?B* Max shift error factor: PEF_13C?F> Maximum number of nuclei per kindJ04) Export/Import Configuration Flags>Exports from DataProc to Mnova:.03) Spectra Referencing4> qNMR reference tolerance?D> qNMR reference position (ERETIC)0> 1H Reference tolerance?.> 1H Reference position2> 13C Reference tolerance?0> 13C Reference positionX02) Quantitative Sample Specific Indications$White-wash ranges:&> Secondary solvent?Q"> Primary solvent?Q<> Sample rotation speed (or 0)<> Presaturation band (if used)@T*> Expected impurities?QN01) Sample Specific Configuration Flags(Helpful Indications:0> Sample purityDataProc1Dstacked, 1HNXn螶RiY7RKlh.>0q;`E{bnd%,ʯAvO>@@Q?@ NMR SpectrumNMR@@@@Xu8      ^:? ??Fs?c*0U2a@ܗpw?c*0U2a kappa?gradient? gamma@ܗ delay?FsG*k*pow(g*G'*d,2)*(D-d/3)scaledG G*k*10scaledGG*kZ8pow(g*G'*d,2)*((4*D-d)/9.87)Z*pow(g*G'*d,2)*(D-d/3)KF-ECBBB @j&L2eMS Shell Dlg 2@>2MNova Default 3&Red-Blue (Gradient) UBϐ}CYM7"|mn*@:U~NXnJwF^=:?^=1?nJwF?~NT?@:?fU?"|m*?YM/?ϐ}C? 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J:/ResearchData/FWN/LIC/NMR_DATA/all_nmr_data/av500/data/nmrafd/nmr/1H_DOSY_gamma-cyclodextrin/19/serData File Name =brukerExpName(datafile(_FILEPATH_), parm.txt(EXPNO), parm.txt(PROCNO))B1H_DOSY_gamma-cyclodextrin.19.ser Title *=Str.trimStr(title())d1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 minsComment  acqus ORIGIN&Bruker BioSpin GmbH Origin  acqus OWNER nmrafd Owner Site  acqus$INSTRUM AvanceInstrument  Author  acqus$SOLVENTD2OSolvent  acqus$TE298.0009Temperature  acqus$PULPROGledbpgp2sPulse Sequence =brukerExperimentType({"pulprog":"acqus($PULPROG)","cnst2":"acqus($CNST[2])"})1DExperiment  acqus$PROBHDPZ109128_0144 (PA BBO 500S2 BBF-H-D-05 Z) Probe  acqus$NS2Number of Scans  acqus$RG101Receiver Gain  acqus $D[1]3 Relaxation Delay  acqus $P[1]14Pulse Width  =brukerPresatFreq(acqus($PULPROG), acqus($SPOFFS[6]), acqus($SFO1), acqus($O1), acqus($SW), procs($OFFSET), fq0list()) .Presaturation Frequency j=brukerAQ(parm.txt(AQ;;;1), acqus($SW_h), acqus($TD))1.31072 Acquisition Time v=brukerDate2(acqus($DATE), parm.txt(Date_), parm.txt(Time))&2024-02-12T12:16:52 Acquisition Date  acqus_LASTMODIFIED_&2024-02-12T12:23:53"Modification Date  Class   %100 Purity  0 Spectrum Quality  titleTitle by User 500.13250065,Spectrometer Frequency  6250.00000000003Spectral Width "-624.349999998243 Lowest Frequency 1HNucleus .=Utl.div(acqus($TD), 2)8192Acquired Size  65536Spectral Size  $0.0953674316406255 $Digital Resolution $Absolute ReferenceUuxnmr.par%*L%m%x]ks:9#;Igm|'i iCM':b ѫэ[zj1Z@7=sc>k,ܭ PKSA>}* TQUAIMLegݎ([]ovfQg}vv{v| Br]'$=;sKP߁L(?-Wb%a3yy3b&9dX_s/5H 5 "q5&^ngwWIi ڶ<^4ڒ¶8]ui ugsӹ҄ 9G)aP ]g)R%WO!&#|HR~pӍvGbKI@E{UTdOWPT::xTKᰂ> -sw9wz åLM.]LўldjȜIܛ?(n\^J﬇.@o(}}xzpxЋKwmE3Hz^VrcޗM..z/ޏ#nQWQru/]_Y|8xe4qnN{W$j RM$7Qͨ'`Arlj2'.ӸX 7ۚtM_G{aq_"Jq@-fqs4^GKM+.޳^$I(lGԗjJqX/%jHּvIK6@ȝιSg6$:t~"`,lAyhn.AQPb;JA V,BdUm$B(EpP,"H"rR, Ex ({Ʀbnp17\ .sܤeHTDUE$ *CHʃS$S$STlbŦ/ CjO!B2/`:y_KB*Lާ7I{O<܌_.m #fga9l9è: Nr=s ڏ%X=u2iH/op~ 'G l N' n N.89nĆ丑nꂓFn N.89nԆi7g689jMmpr4.ii\6qӸljq'M㲩 NeS7˦689nMmpiеQӸljq'M㲩 >7W684NSjOM >5G684$XŽpid?w_rKU`{츟w-[f[bte IkB( ]đ,_U2dB c$ٟq IQ8Rů4df_ kW[5+Yx /[#v`:[߼="q*0A H2iH!o* $%]Yd_Q/ )$0Z%vi6 P #-$"`KD%DGx']!) rUA(}R×] )԰RܰRa.8+bJ]p8Vp +uXQVñ6cݰRkjK_S_S_S_S_S'%i)IIiIIiIIiܚIIiIIia̺jtwy9`9ec4>-wne 4EHy)N1߁4Z7ڷȸ^}mAl{m|(407tLsi­DjnbNs}wSicѳ_65,ni/o񆔇+EEqyQX^T*/*UʋEES]"Jڲ"I"X<<<<J墌z7u@dՄL=~=>~̜yDDM}kuȖ"2_ Qb֤Z;wk+qqY!͕;0R@`RW+'-WHHP L "B!ZO,F 6V05[+ѦqDq4 H/>}Y>SIi7iy~Nj_~W ?\y :#Uz/YյV| >HBs! 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J:/ResearchData/FWN/LIC/NMR_DATA/all_nmr_data/av500/data/nmrafd/nmr/1H_DOSY_gamma-cyclodextrin/19/serData File Name =brukerExpName(datafile(_FILEPATH_), parm.txt(EXPNO), parm.txt(PROCNO))B1H_DOSY_gamma-cyclodextrin.19.ser Title *=Str.trimStr(title())d1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 minsComment  acqus ORIGIN&Bruker BioSpin GmbH Origin  acqus OWNER nmrafd Owner Site  acqus$INSTRUM AvanceInstrument  Author  acqus$SOLVENTD2OSolvent  acqus$TE298.0009Temperature  acqus$PULPROGledbpgp2sPulse Sequence =brukerExperimentType({"pulprog":"acqus($PULPROG)","cnst2":"acqus($CNST[2])"})1DExperiment  acqus$PROBHDPZ109128_0144 (PA BBO 500S2 BBF-H-D-05 Z) Probe  acqus$NS2Number of Scans  acqus$RG101Receiver Gain  acqus $D[1]3 Relaxation Delay  acqus $P[1]14Pulse Width  =brukerPresatFreq(acqus($PULPROG), acqus($SPOFFS[6]), acqus($SFO1), acqus($O1), acqus($SW), procs($OFFSET), fq0list()) .Presaturation Frequency j=brukerAQ(parm.txt(AQ;;;1), acqus($SW_h), acqus($TD))1.31072 Acquisition Time v=brukerDate2(acqus($DATE), parm.txt(Date_), parm.txt(Time))&2024-02-12T12:16:52 Acquisition Date  acqus_LASTMODIFIED_&2024-02-12T12:23:53"Modification Date  Class   %100 Purity  0 Spectrum Quality  titleTitle by User 500.13250065,Spectrometer Frequency  6250.00000000003Spectral Width "-624.349999998243 Lowest Frequency 1HNucleus .=Utl.div(acqus($TD), 2)8192Acquired Size  65536Spectral Size  $0.0953674316406255 $Digital Resolution $Absolute ReferenceUuxnmr.par%*L%m%x]ks:9#;Igm|'i iCM':b ѫэ[zj1Z@7=sc>k,ܭ PKSA>}* TQUAIMLegݎ([]ovfQg}vv{v| Br]'$=;sKP߁L(?-Wb%a3yy3b&9dX_s/5H 5 "q5&^ngwWIi ڶ<^4ڒ¶8]ui ugsӹ҄ 9G)aP ]g)R%WO!&#|HR~pӍvGbKI@E{UTdOWPT::xTKᰂ> -sw9wz åLM.]LўldjȜIܛ?(n\^J﬇.@o(}}xzpxЋKwmE3Hz^VrcޗM..z/ޏ#nQWQru/]_Y|8xe4qnN{W$j RM$7Qͨ'`Arlj2'.ӸX 7ۚtM_G{aq_"Jq@-fqs4^GKM+.޳^$I(lGԗjJqX/%jHּvIK6@ȝιSg6$:t~"`,lAyhn.AQPb;JA V,BdUm$B(EpP,"H"rR, Ex ({Ʀbnp17\ .sܤeHTDUE$ *CHʃS$S$STlbŦ/ CjO!B2/`:y_KB*Lާ7I{O<܌_.m #fga9l9è: Nr=s ڏ%X=u2iH/op~ 'G l N' n N.89nĆ丑nꂓFn N.89nԆi7g689jMmpr4.ii\6qӸljq'M㲩 NeS7˦689nMmpiеQӸljq'M㲩 >7W684NSjOM >5G684$XŽpid?w_rKU`{츟w-[f[bte IkB( ]đ,_U2dB c$ٟq IQ8Rů4df_ kW[5+Yx /[#v`:[߼="q*0A H2iH!o* $%]Yd_Q/ )$0Z%vi6 P #-$"`KD%DGx']!) rUA(}R×] )԰RܰRa.8+bJ]p8Vp +uXQVñ6cݰRkjK_S_S_S_S_S'%i)IIiIIiIIiܚIIiIIia̺jtwy9`9ec4>-wne 4EHy)N1߁4Z7ڷȸ^}mAl{m|(407tLsi­DjnbNs}wSicѳ_65,ni/o񆔇+EEqyQX^T*/*UʋEES]"Jڲ"I"X<<<<J墌z7u@dՄL=~=>~̜yDDM}kuȖ"2_ Qb֤Z;wk+qqY!͕;0R@`RW+'-WHHP L "B!ZO,F 6V05[+ѦqDq4 H/>}Y>SIi7iy~Nj_~W ?\y :#Uz/YյV| >HBs! 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J:/ResearchData/FWN/LIC/NMR_DATA/all_nmr_data/av500/data/nmrafd/nmr/1H_DOSY_gamma-cyclodextrin/19/serData File Name =brukerExpName(datafile(_FILEPATH_), parm.txt(EXPNO), parm.txt(PROCNO))B1H_DOSY_gamma-cyclodextrin.19.ser Title *=Str.trimStr(title())d1H NMR av500; gamma-Cyclodextrin (5mM) in D2O @ 298K 2D DOSY ; ledbpgp2s ns = 2 d1 = 3 sec ramp from 5% till 95% td1 = 32 slices linear d20 =180msec p30 = 1200 usec expt = 5 minsComment  acqus ORIGIN&Bruker BioSpin GmbH Origin  acqus OWNER nmrafd Owner Site  acqus$INSTRUM AvanceInstrument  Author  acqus$SOLVENTD2OSolvent  acqus$TE298.0009Temperature  acqus$PULPROGledbpgp2sPulse Sequence =brukerExperimentType({"pulprog":"acqus($PULPROG)","cnst2":"acqus($CNST[2])"})1DExperiment  acqus$PROBHDPZ109128_0144 (PA BBO 500S2 BBF-H-D-05 Z) Probe  acqus$NS2Number of Scans  acqus$RG101Receiver Gain  acqus $D[1]3 Relaxation Delay  acqus $P[1]14Pulse Width  =brukerPresatFreq(acqus($PULPROG), acqus($SPOFFS[6]), acqus($SFO1), acqus($O1), acqus($SW), procs($OFFSET), fq0list()) .Presaturation Frequency j=brukerAQ(parm.txt(AQ;;;1), acqus($SW_h), acqus($TD))1.31072 Acquisition Time v=brukerDate2(acqus($DATE), parm.txt(Date_), parm.txt(Time))&2024-02-12T12:16:52 Acquisition Date  acqus_LASTMODIFIED_&2024-02-12T12:23:53"Modification Date  Class   %100 Purity  0 Spectrum Quality  titleTitle by User 500.13250065,Spectrometer Frequency  6250.00000000003Spectral Width "-624.349999998243 Lowest Frequency 1HNucleus .=Utl.div(acqus($TD), 2)8192Acquired Size  65536Spectral Size  $0.0953674316406255 $Digital Resolution $Absolute ReferenceUuxnmr.par%*L%m%x]ks:9#;Igm|'i iCM':b ѫэ[zj1Z@7=sc>k,ܭ PKSA>}* TQUAIMLegݎ([]ovfQg}vv{v| Br]'$=;sKP߁L(?-Wb%a3yy3b&9dX_s/5H 5 "q5&^ngwWIi ڶ<^4ڒ¶8]ui ugsӹ҄ 9G)aP ]g)R%WO!&#|HR~pӍvGbKI@E{UTdOWPT::xTKᰂ> -sw9wz åLM.]LўldjȜIܛ?(n\^J﬇.@o(}}xzpxЋKwmE3Hz^VrcޗM..z/ޏ#nQWQru/]_Y|8xe4qnN{W$j RM$7Qͨ'`Arlj2'.ӸX 7ۚtM_G{aq_"Jq@-fqs4^GKM+.޳^$I(lGԗjJqX/%jHּvIK6@ȝιSg6$:t~"`,lAyhn.AQPb;JA V,BdUm$B(EpP,"H"rR, Ex ({Ʀbnp17\ .sܤeHTDUE$ *CHʃS$S$STlbŦ/ CjO!B2/`:y_KB*Lާ7I{O<܌_.m #fga9l9è: Nr=s ڏ%X=u2iH/op~ 'G l N' n N.89nĆ丑nꂓFn N.89nԆi7g689jMmpr4.ii\6qӸljq'M㲩 NeS7˦689nMmpiеQӸljq'M㲩 >7W684NSjOM >5G684$XŽpid?w_rKU`{츟w-[f[bte IkB( ]đ,_U2dB c$ٟq IQ8Rů4df_ kW[5+Yx /[#v`:[߼="q*0A H2iH!o* $%]Yd_Q/ )$0Z%vi6 P #-$"`KD%DGx']!) rUA(}R×] )԰RܰRa.8+bJ]p8Vp +uXQVñ6cݰRkjK_S_S_S_S_S'%i)IIiIIiIIiܚIIiIIia̺jtwy9`9ec4>-wne 4EHy)N1߁4Z7ڷȸ^}mAl{m|(407tLsi­DjnbNs}wSicѳ_65,ni/o񆔇+EEqyQX^T*/*UʋEES]"Jڲ"I"X<<<<J墌z7u@dՄL=~=>~̜yDDM}kuȖ"2_ Qb֤Z;wk+qqY!͕;0R@`RW+'-WHHP L "B!ZO,F 6V05[+ѦqDq4 H/>}Y>SIi7iy~Nj_~W ?\y :#Uz/YյV| >HBs! 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